固溶温度对GH4710合金显微组织和硬度的影响

    Effects of Solution Temperature on Microstructure and Hardness of GH4710 Alloy

    • 摘要: 采用光学显微镜(OM)、扫描电镜(SEM)等方法研究了固溶温度对GH4710合金显微组织和硬度的影响。结果显示:GH4710合金在经过4 h过固溶处理后,该合金的平均晶粒尺寸随固溶温度升高而逐渐增大,晶界平直化程度逐渐增加,这与一次γ'相在过固溶温度下回溶至基体而无法钉扎晶界有关;由于在固溶冷却过程中的过冷度较小,因此二次γ'相的析出未呈现规律性;三次γ'相形貌变化不大,一直保持椭球状,三次γ'相的平均粒径先减小再增大,当固溶温度为1160℃时,三次γ'相的粒径为最小值;三次γ'相的单位面积分数和显微硬度呈现先升高再降低的趋势,当固溶温度为1170℃时,两者皆达最大值。晶粒尺寸的变化与该合金中一次γ'相的变化有关,GH4710合金硬度的变化与该合金中三次γ'相的分布有关。阐明了一次γ'相和三次γ'相在GH4710合金中的作用机理,为该合金的组织性能调控提供了理论依据。

       

      Abstract: The effects of solution temperature on the microstructure and hardness of GH4710 alloy were studied by optical microscopy(OM) and scanning electron microscopy(SEM).The results show that the average grain size of GH4710 alloy increases gradually with the increase of solution temperature, and the degree of grain boundary flatness increases gradually, which is related to the fact that the primary γ' phase is dissolved back into the matrix at the solution temperature and the grain boundary cannot be cemented. Due to the small degree of overcooling during solution cooling, the precipitation of the secondary γ'phase does not show regularity.The morphology of the tertiary γ' phase does not change much, and it has always maintained an ellipsoid shape. The average particle size of the tertiary γ' phase first decreases and then increases. When the solution temperature is 1160 ℃, the particle size of the tertiary γ' phase is the minimum. The unit area fraction and microhardness of the tertiary γ' phase increased first and then decreased, and both reached the maximum value when the solution temperature is 1170 ℃.The change of grain size is related to the change of primary γ' phase in the alloy, and the change of hardness of GH4710 alloy is related to the distribution of the tertiary γ' phase in the alloy. The mechanism of the primary γ' phase and tertiary γ' phase in GH4710 alloy is clarified, it provides a theoretical basis for the regulation of the microstructure and properties of the alloy.

       

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