回火处理对Fe73.5-xCoxCu1Nb3Si13.5B9非晶合金各向异性的影响

    Effect of Tempering Treatment on Anisotropy of Fe73.5-xCoxCu1Nb3Si13.5B9 Amorphous Alloys

    • 摘要: 采用焦耳热处理的方式,对Fe73.5-xCoxCu1Nb3Si13.5B9x=0,10和36.75)非晶合金在一定的电流密度和不同大小的外应力(σ=30~350 MPa)下作用10 s进行退火处理。通过测量磁滞回线,确定了退火样品的应力感生横向各向异性常数K随退火应力的变化。为了进一步研究这一磁性能的稳定性,将x=0和x=10两种组分的退火样品分别在恒定电流下进行了不同时间的回火处理。结果表明:应力感生横向各向异性常数K随外应力的增加而线性增大,这一关系与Herzer的背应力理论一致;K随回火时间的变化均呈现出短时间内快速下降、稍后缓慢减小的趋势。理论分析认为,短时间的变化归因于退火过程产生的内应力随回火时间的松弛,而长时间的变化可用结构弛豫的流变单元模型来解释。

       

      Abstract: Fe73.5-xCoxCu1 Nb3 Si13.5B9x=0, 10 and 36.75) amorphous alloys were annealed with joule-heat treatment under the action of tensile stress(σ=30-350 MPa) for 10 s. The changes of stress-induced transverse anisotropy constant K, with σwere determined by the measurement of hysteresis loop. In order to study the stability of the magnetic hystersis loop, annealed samples of x=0 and x=10 were tempered at a constant annealing current for different tempering time. It is found that the proportional relation between K and σ is observed in three composition samples, which agrees to the tensile back-stress model proposed by Herzer. Additionally, K decreases rapidly in a short time and then decreases slowly with the increase of t. The change in short-time can be attributed to the relaxation of internal stress with time during annealing, and the long-time behavior can be explained by the flow unit model.

       

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